Manufacturers

Muby Chemicals and a few more manufacturing units are owned by Kamdar Family. Mubychem Group is the pioneer manufacturer of Calcium Sulfate or Sulphate etc. in India. Established in 1976, we have led a quality revolution across our product range. Mubychem group has several manufacturing facilities spread across Western India. Our associated facility is Food & Drug Administration (FDA) GMP approved to manufacture a wide range of pharmaceutical excipients and food chemicals. We have ISO-9001-2008 Certification ISO-22000-2005 HACCP Certification, Kosher and Halal Certification. We have European "Reach" Registration for exports.

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MSDS of Calcium Sulfate Sulphate Manufacturers
Calcium Sulfate IP BP USP FCC ACS Manufacturers

Calcium Sulfate USP FCC ACS Calcium Sulphate BP Manufacturers

Calcium Sulfate or Calcium Sulphate is offered as commercial pure Dihydrate, Hemihydrate or Anhydrous and as Pharmaceutical Grade.

Calcium Sulphate as per British Pharmacopoeia

Calcium Sulphate BP Dihydrate

Calcium Sulfate Dihydrate

CaSO4-2H2O --172.2
Action and use
Excipient.

DEFINITION
Content

98.0 per cent to 102.0 per cent of CaSO4-2H2O i.e. Calcium Sulphate Dihydrate or Calcium Sulfate Dihydrate.

CHARACTERS
Appearance

White or almost white fine powder.
Solubility
Very slightly soluble in water, practically insoluble in ethanol (96 per cent).
TESTS Solution S
Dissolve 1.0 g in 50 ml of a 10 per cent V/V solution of hydrochloric acid R by heating at 50C for 5 min. Allow to cool.
Acidity or alkalinity
Shake 1.5 g with 15 ml of carbon dioxide-free water for 5 min. Allow to stand for 5 min and filter. To 10 ml of the filtrate add 0.1 ml of phenolphthalein solution and 0.25 ml of 0.01 M sodium hydroxide . The solution is red. Add 0.30 ml of 0.01 M hydrochloric acid . The solution is colourless. Add 0.2 ml of methyl red solution. The solution is reddish-orange.
Chlorides
Maximum 300 ppm.
Shake 0.5 g with 15 ml of water R for 5 min. Allow to stand for 15 min and filter. Dilute 5 ml of the filtrate to 15 ml with water.
Arsenic
Maximum 10 ppm, determined on 5 ml of solution S.
Iron
Maximum
100 ppm. To 0.25 g add a mixture of 5 ml of hydrochloric acid R and 20 ml of water R. Heat to boiling, cool and filter.
Heavy metals
Maximum 20 ppm.
To 2.5 g add a mixture of 2 ml of hydrochloric acid R and 15 ml of water R. Heat to boiling. Cool and then add 0.5 ml of phenolphthalein solution R. Cautiously add concentrated ammonia until the colour changes to pink. Add 0.5 ml of glacial acetic acid R and dilute to 25 ml with water R. Filter. 12 ml of the filtrate complies with test A. Prepare the reference solution using lead standard solution (2 ppm Pb).
Loss on ignition
18.0 per cent to 22.0 per cent, determined on 1.000 g by ignition to constant mass at 800 50 C.

ASSAY
Dissolve 0.150 g in 120 ml of water. Carry out the complex o metric titration of calcium.
1 ml of 0.1 M sodium edetate is equivalent to 17.22 mg of CaSO4,2H2O.


Calcium Sulfate per US Pharmacopoeia USP

Calcium Sulfate USP

Also Called Calcium Sulphate USP
CaSO4 136.14
Sulfuric acid, calcium salt (1:1).
Calcium sulfate (1:1) 136.14.
Dihydrate 172.17.
Calcium Sulfate is anhydrous or contains two molecules of water of hydration. It contains not less than 98.0 percent and not more than 101.0 percent of CaSO4 i.e. Calcium Sulfate or Calcium Sulphate, calculated on the dried basis.
Loss on drying Dry it at a temperature not lower than 250 to constant weight: the anhydrous form loses not more than 1.5% of its weight, and the dihydrate loses between 19.0% and 23.0% of its weight.

Iron Dissolve 100 mg in 8 mL of 3 N hydrochloric acid, and dilute with water to 47 mL: the limit is 0.01%.

Heavy metals Mix 2.0 g with 20 mL of water, add 25 mL of 3 N hydrochloric acid, and heat to boiling to dissolve the test specimen. Cool, and add ammonium hydroxide to a pH of 7. Filter, evaporate to a volume of about 25 mL, and re-filter, if necessary, to obtain a clear solution:
the limit is 0.001%.
Assay
Dissolve about 300 mg accurately weighed, in 100 mL of water and 4 mL of 3 N hydrochloric acid. Boil, if necessary, to dissolve, and cool before titrating. While stirring, preferably with a magnetic stirrer, add, in the order named, 0.5 mL of triethanolamine, 300 mg of hydroxy naphthol blue, and, from a 50-mL burette, about 30 mL of 0.05 M edetate disodium VS. Add sodium hydroxide solution (45 in 100) until the initial red color changes to clear blue. Continue to add it drop wise until the color changes to violet, and add an additional 0.5 mL. The pH is between 12.3 and 12.5. Continue the titration drop wise with 0.05 M edetate disodium VS to the appearance of a clear-blue endpoint that persists for not less than 60 seconds. Each mL of 0.05 M edentate disodium is equivalent to 6.807 mg of CaSO4.


Calcium Sulfate as per US Food Chemical Codex FCC

Also Called Calcium Sulphate
CaSO4 - CaSO4-2H2O
Formula wt, anhydrous 136.14
Formula wt, dihydrate 172.18
INS: 516 CAS: anhydrous [7778-18-9]
CAS: dihydrate [10101-41-4]

DESCRIPTION
Calcium Sulfate occurs as a fine, white to slightly yellow-white powder. It is anhydrous or contains two molecules of water of hydration.
Function Nutrient; yeast food; dough conditioner; firming agent; sequestrant.

REQUIREMENTS
Assay: Not less than 98.0% of CaSO4 i.e. Calcium Sulphate, calculated on the dried basis.
Fluoride: Not more than 0.003%.
Lead: Not more than 2 mg/kg.
Loss on Drying: Anhydrous: Not more than 1.5%; Dihydrate: Between 19.0% and 23.0%.
Selenium: Not more than 0.003%.

TESTS
Assay Dissolve 250 mg of sample, accurately weighed, in 100 mL of water and 4 mL of 2.7 N hydrochloric acid, boil to effect solution, and cool. While stirring, preferably with a magnetic stirrer, add about 30 mL of 0.05 M disodium EDTA from a 50-mL burette, then add 25 mL of 1 N sodium hydroxide and 300 mg of hydroxy naphthol blue indicator, and continue the titration to a blue endpoint. Each milliliter of 0.05 M disodium EDTA is equivalent to 6.807 mg of CaSO4.


Reagent: Calcium Sulphate Dihydrate as per ACS specifications
American Chemical Society Reagent Grade
Calcium Sulfate Dihydrate ACS

Calcium Sulphate Dihydrate ACS

CaSO4 -2H2O
Formula Wt 172.17
CAS Number 10101-41-4

REQUIREMENTS
Assay: 98.0-102.0% CaSO4-2H2O

MAXIMUM ALLOWABLE
Insoluble in dilute hydrochloric acid: 0.02%
Chloride (Cl): 0.005%
Nitrate (NO3): Passes test
Carbonate (CO3): Passes test
Heavy metals (as Pb): 0.002%
Iron (Fe): 0.001%
Magnesium (Mg): 0.02%
Potassium (K): 0.005%
Sodium (Na): 0.02%
Strontium (Sr): 0.05%

Calcium Sulphate Sulfate Manufacturers
Calcium Sulfate

Calcium Sulfate USP FCC ACS manufacturers or
Calcium Sulphate BP IP manufacturers:

MUBY CHEMICALS
S-8, SARIFA MANSION, 2ND FLANK ROAD, CHINCHBUNDER, MUMBAI 400009, INDIA
TEL: (OFFICE) 91-22-23770100, 23774610, 23726950, 23723564. FAX: 91-22-23728264

e-mail: info@mubychem.com

USA & Canadian Customers may e-mail: usa@mubychem.com

Copyright and Usual Disclaimer is Applicable.
Last updated: 03 June, 2014.

Commercial Pure & BP USP NF IP ACS AR Analytical Reagent, FCC Food Grades
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Calcium Hydroxide Calcium Oxide; Lime Calcium Sulfate
Calcium D Glucarate Saccharate Chromic Chloride; Chromium Chloride Iron Sulphide or Ferrous Sulfide
Gentian Violet Magnesium Chloride Pharmaceutical grade Magnesium Sulfate
Maleic Acid Manganese Chloride Manganese Sulfate
Mono/Di Ammonium Phosphate Mono/Di/Tri Sodium Phosphate Magnesium Chloride Anhydrous & Hexahydrate
Methylene Blue Mono/Di/Tri Potassium Phosphate PCB Etchant or Ammonical Etchant
Potassium Bromide Potassium Chloride Potassium Chloride Pharmaceutical grade
Sodium Acetate Sodium Acetate Pharmaceutical grade Sodium Bicarbonate
Sodium Bromide Sodium Chloride Sodium Hydroxide
Sodium Diacetate Sodium Hydroxymethanesulphonate Formaldehyde Bisulphite
Sodium Thiosulphate Sodium Thiosulfate Pharmaceutical grade Zinc Chloride
Zinc Chloride Pharmaceutical grade Zinc Ammonium Chloride Flux Zinc Sulphate or Zinc Sulfate

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